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Index Experimental Pages 1-13 References from Experimental Page 14
BibTeX
@MISC{Adriaenssens_indexexperimental,
author = {V. Adriaenssens and Carolyn A. Austin and Mairi Gibson and David Smith and Richard C and Ref No. O},
title = {Index Experimental Pages 1-13 References from Experimental Page 14},
year = {}
}
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Abstract
Scanned spectra in numerical order Pages 15-27 Experimental All reactons under an inert atmosphere were carried out using oven dried or flame dried glassware. Solutions were added via syringe. THF was freshly distilled from sodium benzophenone. Dichloromethane, and triethyl phosphite were distilled from CaH2 prior to use. Petroleum ether refers to the fraction boiling at 40-60 °C. Reagents were obtained from commercial suppliers and used without further purification unless otherwise stated. The solid phase reactions were carried out in normal glassware, but with the resin (particle size = 150-300 µm diameter) contained within porous polypropylene reactors that had an internal volume of 2.4 mL, and a pore size of 74 µm. Purification by column chromatography was carried out using silica gel, mesh size 35-70 µm. as the stationary phase. 1H and 13C NMR spectra were obtained on a Bruker DPX/400 spectrometer operating at 400 and 100 MHz respectively. All coupling constants are measured in Hz. DEPT was used to assign the signals in the 13C NMR spectra as C, CH, CH2 or CH3. Mass spectra (MS) were recorded on a Jeol JMS700 (MStation) spectrometer. Infra-red (IR) spectra were obtained on a Perkin-Elmer 983 spectrophotometer. A Golden GateTM attachment that uses a type IIa diamond as
Keyphrases
experimental page index experimental page 1-13 reference nmr spectrum pore size solid phase reaction column chromatography commercial supplier particle size 150-300 diameter internal volume mesh size 35-70 golden gatetm attachment normal glassware mass spectrum stationary phase coupling constant sodium benzophenone jeol jms700 silica gel triethyl phosphite porous polypropylene reactor spectrometer operating type iia diamond inert atmosphere bruker dpx
